[(C(1-adamantyl))2P₄(W(CO)5)2]

Base Information

• Chemical Name: [(C(1-adamantyl))2P₄(W(CO)5)2]
• CAS No.: 1138340-24-5
• Molecular Formula: C₃₂H₃₀O₁₀P₄W₂
• Molecular Weight: 1066.18
• Mol file: 1138340-24-5.mol

Synonyms:

Chemical Property of [(C(1-adamantyl))2P₄(W(CO)5)2]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of [(C(1-adamantyl))2P₄(W(CO)5)2]

There total 1 articles about [(C(1-adamantyl))2P₄(W(CO)5)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

[(W(CO)5)2P3(C(1-adamantyl)O)Nb(N(CH2(tert-butyl))(3,5-(methyl)2C6H3))3] + 1-adamantylphosphaacetylene (101055-70-3) → [ONb(N(CH2(tert-butyl))(3,5-(methyl)2C6H3))3] + [(C(1-adamantyl))2P4(W(CO)5)2] (1138340-24-5)

Guidance literature:

In benzene; under anhydrous and oxygen-free conditions; mixed, dissolved in benzene,soln. heated at 35°C for 3.5 h, filtered through celite, evapd. to dryness; Nb compd. extd. with pentane, remaining solid collected on frit, washed with pentane, dried in vac.;

DOI:10.1002/anie.200804432

upstream raw materials:

1-adamantylphosphaacetylene