1,3-bis(2-(3,5-bis(bromomethyl)phenyl)ethyl)benzene

Base Information

Chemical Name:1,3-bis(2-(3,5-bis(bromomethyl)phenyl)ethyl)benzene
CAS No.:1263078-33-6
Molecular Formula:C₂₆H₂₆Br₄
Molecular Weight:658.108
Hs Code.:

Synonyms:

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Chemical Property of 1,3-bis(2-(3,5-bis(bromomethyl)phenyl)ethyl)benzene

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Technology Process of 1,3-bis(2-(3,5-bis(bromomethyl)phenyl)ethyl)benzene

There total 6 articles about 1,3-bis(2-(3,5-bis(bromomethyl)phenyl)ethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: C₂₆H₃₀O₄

: 1263078-33-6
1,3-bis(2-(3,5-bis(bromomethyl)phenyl)ethyl)benzene

Guidance literature:: With hydrogen bromide; In acetic acid; for 0.166667h; Reflux; Inert atmosphere;
DOI:10.1071/CH10356

Reference yield:

: 1201635-31-5
1,3-bis(3,5-bis(methoxycarbonyl)phenylethynyl)benzene

: 1263078-33-6
1,3-bis(2-(3,5-bis(bromomethyl)phenyl)ethyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: palladium on carbon; hydrogen / acetic acid; benzene / 16 h / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 22.75 h / 0 - 20 °C / Inert atmosphere

3: hydrogen bromide / acetic acid / 0.17 h / Reflux; Inert atmosphere

With lithium aluminium tetrahydride; palladium on carbon; hydrogen bromide; hydrogen; In tetrahydrofuran; acetic acid; benzene;
DOI:10.1071/CH10356

Reference yield:

: 168619-21-4
3,5-bis(methoxycarbonyl)phenyl trifluoromethanesulfonate

: 1263078-33-6
1,3-bis(2-(3,5-bis(bromomethyl)phenyl)ethyl)benzene

Guidance literature:: Multi-step reaction with 6 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene / benzene / 20.16 h / 20 °C / Inert atmosphere

2: potassium carbonate / methanol / 1.5 h / 20 °C / Inert atmosphere

3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene / benzene / 3.08 h / 20 °C / Inert atmosphere

4: palladium on carbon; hydrogen / acetic acid; benzene / 16 h / 20 °C

5: lithium aluminium tetrahydride / tetrahydrofuran / 22.75 h / 0 - 20 °C / Inert atmosphere

6: hydrogen bromide / acetic acid / 0.17 h / Reflux; Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; lithium aluminium tetrahydride; palladium on carbon; hydrogen bromide; hydrogen; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; acetic acid; benzene; 1: Sonogashira reaction;
DOI:10.1071/CH10356