Technology Process of C27H37N6O9P
There total 10 articles about C27H37N6O9P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: sodium methylate / 24 h / 20 °C
2.1: pyridine / 16 h / 20 °C
3.1: pyridine / dichloromethane / 5 h / 20 °C
4.1: water; 4-methylmorpholine N-oxide / osmium(VIII) oxide / tert-butyl alcohol; tetrahydrofuran / 16 h / 20 °C
5.1: sodium periodate / water; tetrahydrofuran / 3 h / 20 °C
5.2: 1 h / 0 °C
6.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C
7.1: ammonium fluoride / methanol / 5 h / 60 °C
8.1: sodium methylate; methanol / 20 h / 20 °C
9.1: tert-butylmagnesium chloride / tetrahydrofuran / 0.5 h / 20 °C / Cooling with ice
9.2: 4 h / 20 °C
With
pyridine; methanol; ammonium fluoride; sodium periodate; tert-butylmagnesium chloride; water; sodium methylate; sodium hydride; 4-methylmorpholine N-oxide;
pyridine; osmium(VIII) oxide;
In
tetrahydrofuran; methanol; dichloromethane; water; mineral oil; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 10 steps
1.1: trimethylsilyl trifluoromethanesulfonate; DBN / acetonitrile / 21 h / 0 - 65 °C
2.1: sodium methylate / 24 h / 20 °C
3.1: pyridine / 16 h / 20 °C
4.1: pyridine / dichloromethane / 5 h / 20 °C
5.1: water; 4-methylmorpholine N-oxide / osmium(VIII) oxide / tert-butyl alcohol; tetrahydrofuran / 16 h / 20 °C
6.1: sodium periodate / water; tetrahydrofuran / 3 h / 20 °C
6.2: 1 h / 0 °C
7.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C
8.1: ammonium fluoride / methanol / 5 h / 60 °C
9.1: sodium methylate; methanol / 20 h / 20 °C
10.1: tert-butylmagnesium chloride / tetrahydrofuran / 0.5 h / 20 °C / Cooling with ice
10.2: 4 h / 20 °C
With
pyridine; methanol; ammonium fluoride; sodium periodate; trimethylsilyl trifluoromethanesulfonate; DBN; tert-butylmagnesium chloride; water; sodium methylate; sodium hydride; 4-methylmorpholine N-oxide;
pyridine; osmium(VIII) oxide;
In
tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; mineral oil; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: pyridine / dichloromethane / 5 h / 20 °C
2.1: water; 4-methylmorpholine N-oxide / osmium(VIII) oxide / tert-butyl alcohol; tetrahydrofuran / 16 h / 20 °C
3.1: sodium periodate / water; tetrahydrofuran / 3 h / 20 °C
3.2: 1 h / 0 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C
5.1: ammonium fluoride / methanol / 5 h / 60 °C
6.1: sodium methylate; methanol / 20 h / 20 °C
7.1: tert-butylmagnesium chloride / tetrahydrofuran / 0.5 h / 20 °C / Cooling with ice
7.2: 4 h / 20 °C
With
methanol; ammonium fluoride; sodium periodate; tert-butylmagnesium chloride; water; sodium methylate; sodium hydride; 4-methylmorpholine N-oxide;
pyridine; osmium(VIII) oxide;
In
tetrahydrofuran; methanol; dichloromethane; water; mineral oil; tert-butyl alcohol;