bis(2-hydroxybenzaldehydethiobenzoylhdydrazonato)nickel(II)

Base Information

Chemical Name:bis(2-hydroxybenzaldehydethiobenzoylhdydrazonato)nickel(II)
CAS No.:220706-08-1
Molecular Formula:C₂₈H₂₂N₄NiO₂S₂
Molecular Weight:569.33
Hs Code.:

Synonyms:

Suppliers and Price of bis(2-hydroxybenzaldehydethiobenzoylhdydrazonato)nickel(II)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of bis(2-hydroxybenzaldehydethiobenzoylhdydrazonato)nickel(II)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of bis(2-hydroxybenzaldehydethiobenzoylhdydrazonato)nickel(II)

There total 3 articles about bis(2-hydroxybenzaldehydethiobenzoylhdydrazonato)nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: nickel(II) acetate hydrate

: 89983-79-9
salicylaldehyde thiobenzoyl hydrazone

: 220706-08-1
bis(2-hydroxybenzaldehydethiobenzoylhdydrazonato)nickel(II)

Guidance literature:: With CH₃COONa; In ethanol; water; refluxing a mixt of a soln. of ligand in ethanol with a soln. of metal salt in ethanol/water in the presence of CH3COONa for 30 min; filtration, washing with water and ethanol, drying in vac.; elem. anal.;

Reference yield:

: 89983-79-9
salicylaldehyde thiobenzoyl hydrazone

: 373-02-4,14998-37-9,33025-09-1,94044-50-5,98268-31-6
nickel diacetate

: 220706-08-1
bis(2-hydroxybenzaldehydethiobenzoylhdydrazonato)nickel(II)

Guidance literature:: In methanol; addn. of a soln. of Ni acetate in methanol to a heated soln. of the ligand in methanol, pptn.; filtration (after 1 d), washing (hot methanol), drying (vac.);

Reference yield:

: 89983-79-9
salicylaldehyde thiobenzoyl hydrazone

: 373-02-4,14998-37-9,33025-09-1,94044-50-5,98268-31-6
nickel diacetate

: 220706-08-1
Ni(C₆H₄(OH)CHNNCSC₆H₅)2

Guidance literature:: In methanol; a soln. of the ligand is added to a soln. of Ni-acetate with stirring;; pptd.; filtered; washed with hot methanol; dried; elem. anal.;;