Yb⁽³⁺⁾*C₂H₄(NC₃H₆)2(NC₂H₄)2^(2-)*SC₆H₄CH₃^(1-)=[Yb(C₂H₄(NC₃H₆)2(NC₂H₄)2)(SC₆H₄CH₃)]

Base Information

• Chemical Name: Yb⁽³⁺⁾*C₂H₄(NC₃H₆)2(NC₂H₄)2^(2-)*SC₆H₄CH₃^(1-)=[Yb(C₂H₄(NC₃H₆)2(NC₂H₄)2)(SC₆H₄CH₃)]
• CAS No.: 898290-16-9
• Molecular Formula: C₇H₇S*C₁₂H₂₄N₄*Yb
• Molecular Weight: 520.588

Synonyms:

Chemical Property of Yb⁽³⁺⁾*C₂H₄(NC₃H₆)2(NC₂H₄)2^(2-)*SC₆H₄CH₃^(1-)=[Yb(C₂H₄(NC₃H₆)2(NC₂H₄)2)(SC₆H₄CH₃)]

Chemical Property:

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Safty Information:

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MSDS Files:

Useful:

Technology Process of Yb⁽³⁺⁾*C₂H₄(NC₃H₆)2(NC₂H₄)2^(2-)*SC₆H₄CH₃^(1-)=[Yb(C₂H₄(NC₃H₆)2(NC₂H₄)2)(SC₆H₄CH₃)]

There total 1 articles about Yb⁽³⁺⁾*C₂H₄(NC₃H₆)2(NC₂H₄)2^(2-)*SC₆H₄CH₃^(1-)=[Yb(C₂H₄(NC₃H₆)2(NC₂H₄)2)(SC₆H₄CH₃)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

bis(pentamethylcyclopentadienyl)ytterbium(diethyl ether) + di(p-tolyl) disulfide (103-19-5) + 1,4,8,11-tetraazabicyclo[6.6.2]hexadecane (130701-19-8) → Yb(3+)*C2H4(NC3H6)2(NC2H4)2(2-)*SC6H4CH3(1-)=[Yb(C2H4(NC3H6)2(NC2H4)2)(SC6H4CH3)] (898290-16-9)

Guidance literature:

In toluene; (N2); glovebox; soln. of ligand in toluene was added with stirring to soln. of Yb compd. in toluene; suspn. was stirred for 4 h; soln. of sulfide in toluene was added; soln. was stirred for 2 h; filtered through Celite; layered with hexane; kept overnight; mother liquor decanted; washed (cold toluene, hexane); dried in vac. for several h; mother liquor cooled to -30°C; elem. anal.;

DOI:10.1016/j.ica.2005.11.015

upstream raw materials:

di(p-tolyl) disulfide

1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

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