Technology Process of C23H23IN2
There total 7 articles about C23H23IN2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 0 - 20 ℃;
for 16h;
Inert atmosphere;
DOI:10.1021/jo2025724
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 2,2,6,6-tetramethyl-piperidine; n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere
1.2: 2 h / -78 - 20 °C / Inert atmosphere
2.1: sulfuric acid; acetic acid / water / 16 h / 0 - 120 °C / Inert atmosphere; Reflux
3.1: sulfuric acid; sodium nitrite / water; acetonitrile / 20 °C / Inert atmosphere
4.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C / Inert atmosphere
5.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere
6.1: thionyl chloride / 85 °C / Inert atmosphere
7.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere
With
2,2,6,6-tetramethyl-piperidine; n-butyllithium; thionyl chloride; oxalyl dichloride; sulfuric acid; acetic acid; triethylamine; N,N-dimethyl-formamide; sodium nitrite;
In
tetrahydrofuran; hexane; dichloromethane; water; acetonitrile;
DOI:10.1021/jo2025724
- Guidance literature:
-
Multi-step reaction with 2 steps
1: thionyl chloride / 85 °C / Inert atmosphere
2: triethylamine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere
With
thionyl chloride; triethylamine;
In
dichloromethane;
DOI:10.1021/jo2025724
