Technology Process of C36H36N2O3
There total 7 articles about C36H36N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 7 steps
1.1: N,N-dimethyl-formamide dimethyl acetal / N,N-dimethyl-formamide / 130 °C
1.2: 20 °C
2.1: sodium hydride; potassium iodide / 0 °C / Reflux
3.1: zinc; acetic acid / 80 °C
4.1: sodium hydride / dichloromethane / 0 - 20 °C
5.1: sodium hydroxide / 1,4-dioxane / 80 °C
6.1: HATU; triethylamine / dichloromethane / 20 °C
7.1: hydrogenchloride / ethyl acetate / 20 °C
With
hydrogenchloride; sodium hydride; acetic acid; N,N-dimethyl-formamide dimethyl acetal; triethylamine; HATU; potassium iodide; sodium hydroxide; zinc;
In
1,4-dioxane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.01.004
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydroxide / 1,4-dioxane / 80 °C
2: HATU; triethylamine / dichloromethane / 20 °C
3: hydrogenchloride / ethyl acetate / 20 °C
With
hydrogenchloride; triethylamine; HATU; sodium hydroxide;
In
1,4-dioxane; dichloromethane; ethyl acetate;
DOI:10.1016/j.bmcl.2014.01.004