C₃₂H₃₃F₂N₇O₃

Base Information

Chemical Name:C₃₂H₃₃F₂N₇O₃
CAS No.:1449426-10-1
Molecular Formula:C₃₂H₃₃F₂N₇O₃
Molecular Weight:601.656
Hs Code.:

C<sub>32</sub>H<sub>33</sub>F<sub>2</sub>N<sub>7</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₃₂H₃₃F₂N₇O₃

Chemical Property:

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Technology Process of C₃₂H₃₃F₂N₇O₃

There total 5 articles about C₃₂H₃₃F₂N₇O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1436686-20-2
C₂₁H₃₀N₄O₄

: 1449426-10-1
C₃₂H₃₃F₂N₇O₃

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide; methanol / water / 60 °C

2: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / tetrahydrofuran

With methanol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; lithium hydroxide; In tetrahydrofuran; water;
DOI:10.1016/j.bmcl.2013.04.020

Reference yield:

: 5-oxo-4,5-dihydropyrazolo[1,5-a]pyrimidine-3-carboxylic acid ethyl ester

: 1449426-10-1
C₃₂H₃₃F₂N₇O₃

Guidance literature:: Multi-step reaction with 5 steps

1: phosphorus(V) oxybromide / acetonitrile / 130 °C

2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 20 °C

3: palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C

4: lithium hydroxide; methanol / water / 60 °C

5: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / tetrahydrofuran

With methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; palladium on activated charcoal; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; lithium hydroxide; phosphorus(V) oxybromide; In tetrahydrofuran; water; ethyl acetate; acetonitrile; 2: |Sonogashira Cross-Coupling;
DOI:10.1016/j.bmcl.2013.04.020

Reference yield:

: 1436686-17-7
5-bromopyrazolo[1,5-a]pyrimidine-3-carboxylic acid ethyl ester

: 1449426-10-1
C₃₂H₃₃F₂N₇O₃

Guidance literature:: Multi-step reaction with 4 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 20 °C

2: palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C

3: lithium hydroxide; methanol / water / 60 °C

4: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / tetrahydrofuran

With methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; palladium on activated charcoal; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; lithium hydroxide; In tetrahydrofuran; water; ethyl acetate; 1: |Sonogashira Cross-Coupling;
DOI:10.1016/j.bmcl.2013.04.020