subergorgic acid

Base Information

• Chemical Name: subergorgic acid
• CAS No.: 113429-19-9
• Molecular Formula: C₁₅H₂₀O₃
• Molecular Weight: 248.322
• Mol file: 113429-19-9.mol

Synonyms:

Chemical Property of subergorgic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of subergorgic acid

There total 8 articles about subergorgic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C16H22O2 (131509-90-5) → (+/-)-Subergorgic acid (84607-62-5,97718-45-1,110043-85-1,113429-19-9)

Guidance literature:

Multi-step reaction with 7 steps

1: 67 percent / benzoyl peroxide / Heating

2: 90 percent / K, 18-Crown-6 / toluene / Heating

3: 80 percent / m-CPBA

4: 70 percent / N-cyclohexyl,N-isopropyl amine, MeMgBr

5: 85 percent / SOCl₂, pyridine

6: 85 percent / DMSO, AgBF₄

7: NaClO₂

With pyridine; sodium chlorite; silver tetrafluoroborate; thionyl chloride; 18-crown-6 ether; N-cyclohexylisopropylamine; methylmagnesium bromide; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid; dibenzoyl peroxide; In toluene;

DOI:10.1016/S0040-4039(00)97864-X

Reference yield:

2-(2,5-Dimethyl-phenyl)-2-(2-methyl-but-3-enyl)-[1,3]dioxolane (131509-88-1) → (+/-)-Subergorgic acid (84607-62-5,97718-45-1,110043-85-1,113429-19-9)

Guidance literature:

Multi-step reaction with 8 steps

1: cyclohexane / Irradiation

2: 67 percent / benzoyl peroxide / Heating

3: 90 percent / K, 18-Crown-6 / toluene / Heating

4: 80 percent / m-CPBA

5: 70 percent / N-cyclohexyl,N-isopropyl amine, MeMgBr

6: 85 percent / SOCl₂, pyridine

7: 85 percent / DMSO, AgBF₄

8: NaClO₂

With pyridine; sodium chlorite; silver tetrafluoroborate; thionyl chloride; 18-crown-6 ether; N-cyclohexylisopropylamine; methylmagnesium bromide; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid; dibenzoyl peroxide; In cyclohexane; toluene;

DOI:10.1016/S0040-4039(00)97864-X

Reference yield:

C18H25NO2 (131509-91-6) → (+/-)-Subergorgic acid (84607-62-5,97718-45-1,110043-85-1,113429-19-9)

Guidance literature:

Multi-step reaction with 6 steps

1: 90 percent / K, 18-Crown-6 / toluene / Heating

2: 80 percent / m-CPBA

3: 70 percent / N-cyclohexyl,N-isopropyl amine, MeMgBr

4: 85 percent / SOCl₂, pyridine

5: 85 percent / DMSO, AgBF₄

6: NaClO₂

With pyridine; sodium chlorite; silver tetrafluoroborate; thionyl chloride; 18-crown-6 ether; N-cyclohexylisopropylamine; methylmagnesium bromide; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid; In toluene;

DOI:10.1016/S0040-4039(00)97864-X

upstream raw materials:

Subergorgic aldehyde

C₁₇H₂₆O₃

(3S,3aR,5aR,8S)-7-Chloromethyl-3,5a,8-trimethyl-3,3a,4,5,5a,8-hexahydro-2H-cyclopenta[c]pentalen-1-one

C₁₆H₂₂O₂