C₂₃H₂₃NO₃*ClH

Base Information

Chemical Name:C₂₃H₂₃NO₃*ClH
CAS No.:1228098-91-6
Molecular Formula:C₂₃H₂₃NO₃*ClH
Molecular Weight:397.901
Hs Code.:

C<sub>23</sub>H<sub>23</sub>NO<sub>3</sub>*ClH

Synonyms:

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Chemical Property of C₂₃H₂₃NO₃*ClH

Chemical Property:

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Technology Process of C₂₃H₂₃NO₃*ClH

There total 4 articles about C₂₃H₂₃NO₃*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1228098-87-0
C₂₃H₂₈BrNO₄

: 1228098-91-6
C₂₃H₂₃NO₃*ClH

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium diacetate; triphenylphosphine / isopropyl alcohol / 0.5 h / 20 °C / Inert atmosphere

1.2: 16 h / Inert atmosphere; Reflux

2.1: hydrogenchloride; water / diethyl ether

With hydrogenchloride; water; palladium diacetate; triphenylphosphine; In diethyl ether; isopropyl alcohol; 1.1: Suzuki-Miyaura coupling reaction / 1.2: Suzuki-Miyaura coupling reaction;
DOI:10.1007/s00044-010-9356-8

Reference yield:

: 3213-28-3
3,5-dimethoxyphenethylamine

: 1228098-91-6
C₂₃H₂₃NO₃*ClH

Guidance literature:: Multi-step reaction with 6 steps

1.1: diethyl cyanophosphonate; triethylamine / N,N-dimethyl-formamide

2.1: trichlorophosphate / acetonitrile

3.1: sodium tetrahydroborate / methanol; water

4.1: sodium hydroxide / tetrahydrofuran; dichloromethane

5.1: palladium diacetate; triphenylphosphine / isopropyl alcohol / 0.5 h / 20 °C / Inert atmosphere

5.2: 16 h / Inert atmosphere; Reflux

6.1: hydrogenchloride; water / diethyl ether

With hydrogenchloride; sodium tetrahydroborate; diethyl cyanophosphonate; water; palladium diacetate; triethylamine; triphenylphosphine; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile; 2.1: Bischler-Napieralski reaction / 5.1: Suzuki-Miyaura coupling reaction / 5.2: Suzuki-Miyaura coupling reaction;
DOI:10.1007/s00044-010-9356-8

Reference yield:

: 1228098-84-7
C₁₈H₂₀BrNO₃

: 1228098-91-6
C₂₃H₂₃NO₃*ClH

Guidance literature:: Multi-step reaction with 5 steps

1.1: trichlorophosphate / acetonitrile

2.1: sodium tetrahydroborate / methanol; water

3.1: sodium hydroxide / tetrahydrofuran; dichloromethane

4.1: palladium diacetate; triphenylphosphine / isopropyl alcohol / 0.5 h / 20 °C / Inert atmosphere

4.2: 16 h / Inert atmosphere; Reflux

5.1: hydrogenchloride; water / diethyl ether

With hydrogenchloride; sodium tetrahydroborate; water; palladium diacetate; triphenylphosphine; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; isopropyl alcohol; acetonitrile; 1.1: Bischler-Napieralski reaction / 4.1: Suzuki-Miyaura coupling reaction / 4.2: Suzuki-Miyaura coupling reaction;
DOI:10.1007/s00044-010-9356-8