Technology Process of C24H31N5O3S
There total 5 articles about C24H31N5O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C18H21N5OS;
With
sodium hydride;
In
acetonitrile;
at 25 ℃;
for 1h;
Inert atmosphere;
bromoacetic acid tert-butyl ester;
In
acetonitrile;
at 25 ℃;
for 3.5h;
regioselective reaction;
Inert atmosphere;
DOI:10.1039/c3cc37265k
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N,N-dimethyl-formamide / 2 h / 50 °C / Inert atmosphere
2.1: sodium hydride / acetonitrile / 1 h / 25 °C / Inert atmosphere
2.2: 3.5 h / 25 °C / Inert atmosphere
With
sodium hydride;
In
N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c3cc37265k
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 8 h / 70 °C / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 25 °C / Inert atmosphere
2.2: 13 h / 25 °C / Inert atmosphere
3.1: ammonium hydroxide; ammonia / water; methanol / 40 h / 55 °C / Inert atmosphere
4.1: N,N-dimethyl-formamide / 2 h / 50 °C / Inert atmosphere
5.1: sodium hydride / acetonitrile / 1 h / 25 °C / Inert atmosphere
5.2: 3.5 h / 25 °C / Inert atmosphere
With
ammonium hydroxide; N-Bromosuccinimide; ammonia; sodium hydride; dibenzoyl peroxide;
In
methanol; tetrachloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c3cc37265k
