cyclopentadienylcobalt carbonyl(1,2-bis(diphenylphosphino)ethane)

Base Information

Chemical Name:cyclopentadienylcobalt carbonyl(1,2-bis(diphenylphosphino)ethane)
CAS No.:113160-76-2
Molecular Formula:C₃₁H₂₇CoOP₂
Molecular Weight:536.495
Hs Code.:

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Chemical Property of cyclopentadienylcobalt carbonyl(1,2-bis(diphenylphosphino)ethane)

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Technology Process of cyclopentadienylcobalt carbonyl(1,2-bis(diphenylphosphino)ethane)

There total 1 articles about cyclopentadienylcobalt carbonyl(1,2-bis(diphenylphosphino)ethane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 12078-25-0,12078-23-8
dicarbonylcyclopentadienylcobalt

: 2071-20-7
bis-diphenylphosphinomethane

: 113160-76-2
cyclopentadienylcobalt carbonyl(1,2-bis(diphenylphosphino)ethane)

Guidance literature:: In benzene; addn. of phosphine to Co-compound in benzene (N2, Schlenk tube technique), stirring for 3 h at 60°C; cooling to room temp., addn. of ether, filtn., washing with ether, recrystn. from benzene/pentane, elem. anal.;

Reference yield: 47.0%

: ammonium hexafluorophosphate

: 113160-76-2
cyclopentadienylcobalt carbonyl(1,2-bis(diphenylphosphino)ethane)

: 113160-78-4
(C₅H₅CoCoCH₃(dppm))PF₆

Guidance literature:: With CH₃I; In benzene; addn. of CH3I to Co-compound in benzene (N2, Schlenk tube technique), stirring for 5 h at room temp., addn. of ether, filtn., washing with ether, dissolving in methanol and addn. of NH4PF6, stirring for 10 min; recrystn. from nitromethane/ether, elem. anal.;