((.eta**⁽⁶⁾-benzenecarboxylate) chromium tricarbonyl)2Zn(5-methyl-3-phenyl pyrazole)2

Base Information

• Chemical Name: ((.eta**⁽⁶⁾-benzenecarboxylate) chromium tricarbonyl)2Zn(5-methyl-3-phenyl pyrazole)2
• CAS No.: 1356337-27-3
• Molecular Formula: C₄₀H₃₀Cr₂N₄O₁₀Zn
• Molecular Weight: 896.081

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Chemical Property of ((.eta**⁽⁶⁾-benzenecarboxylate) chromium tricarbonyl)2Zn(5-methyl-3-phenyl pyrazole)2

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Technology Process of ((.eta**⁽⁶⁾-benzenecarboxylate) chromium tricarbonyl)2Zn(5-methyl-3-phenyl pyrazole)2

There total 1 articles about ((.eta**⁽⁶⁾-benzenecarboxylate) chromium tricarbonyl)2Zn(5-methyl-3-phenyl pyrazole)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(η6-benzoic acid)chromium tricarbonyl (12294-91-6) + zinc(II) acetate dihydrate (5970-45-6) + 3-methyl-5-phenylpyrazole (56426-41-6) → ((.eta**(6)-benzenecarboxylate) chromium tricarbonyl)2Zn(5-methyl-3-phenyl pyrazole)2 (1356337-27-3)

Guidance literature:

In methanol; Zn acetate and pyrazole deriv. dissolved in MeOH, mixt. stirred for 1 h;then soln. of Cr complex added; mixt. stirred for 6 h; CH2Cl2 added; crystd. from CH2Cl2/MeOH mixt.; elem. anal.;

DOI:10.1002/zaac.201100269

upstream raw materials:

(η6-benzoic acid)chromium tricarbonyl

zinc(II) acetate dihydrate

3-methyl-5-phenylpyrazole

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