1,1-dimesityl-2,4-diphenyl-1-germacyclopentadiene

Base Information

• Chemical Name: 1,1-dimesityl-2,4-diphenyl-1-germacyclopentadiene
• CAS No.: 227027-23-8
• Molecular Formula: C₃₄H₃₄Ge
• Molecular Weight: 515.234
• Mol file: 227027-23-8.mol

Synonyms:

Chemical Property of 1,1-dimesityl-2,4-diphenyl-1-germacyclopentadiene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1,1-dimesityl-2,4-diphenyl-1-germacyclopentadiene

There total 1 articles about 1,1-dimesityl-2,4-diphenyl-1-germacyclopentadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

hexamesitylsiladigermirane (136131-68-5) + phenylacetylene (536-74-3) → 1,1-dimesityl-2,4-diphenyl-1-germacyclopentadiene (227027-23-8) + 3-phenyl-1,1,2,2-tetramesityl-1-sila-2-germacyclobutene (227027-21-6) + 2,5-diphenyl-1,1,4,4-tetramesityl-1,4-digermacyclohexa-2,5-diene (227027-22-7)

Guidance literature:

In neat (no solvent); Ar-atmosphere; phenylacetylene as solvent, heating to 105°C for 5h; evapn., chromy. (Chromatotron, 10% CH2Cl2:hexane);

DOI:10.1021/om981017h

upstream raw materials:

hexamesitylsiladigermirane

phenylacetylene