<(1S)-(1,2,4/3,5)-2,3,4-tribenzyloxy-5-benzyloxymethyl-1-cyclohexyl> 2-acetamido-2-deoxy-β-D-glucopyranoside triacetate

Base Information

Chemical Name:<(1S)-(1,2,4/3,5)-2,3,4-tribenzyloxy-5-benzyloxymethyl-1-cyclohexyl> 2-acetamido-2-deoxy-β-D-glucopyranoside triacetate
CAS No.:117509-51-0
Molecular Formula:C₄₉H₅₇NO₁₃
Molecular Weight:867.99
Hs Code.:

Synonyms:

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Chemical Property of <(1S)-(1,2,4/3,5)-2,3,4-tribenzyloxy-5-benzyloxymethyl-1-cyclohexyl> 2-acetamido-2-deoxy-β-D-glucopyranoside triacetate

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Technology Process of <(1S)-(1,2,4/3,5)-2,3,4-tribenzyloxy-5-benzyloxymethyl-1-cyclohexyl> 2-acetamido-2-deoxy-β-D-glucopyranoside triacetate

There total 28 articles about <(1S)-(1,2,4/3,5)-2,3,4-tribenzyloxy-5-benzyloxymethyl-1-cyclohexyl> 2-acetamido-2-deoxy-β-D-glucopyranoside triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117486-50-7,117604-11-2,117604-12-3,117773-05-4
<(1R)-(1,2,4/3,5)-2,3,4-tribenzyloxy-5-benzyloxymethyl-1-cyclohexyl> 2-deoxy-2-(2,4-dinitrophenylamino)-α-D-glucopyranoside triacetate

: 117509-51-0,117604-13-4,117604-14-5,117604-82-7
<(1R)-(1,2,4/3,5)-2,3,4-tribenzyloxy-5-benzyloxymethyl-1-cyclohexyl> 2-acetamido-2-deoxy-α-D-glucopyranoside triacetate

Guidance literature:: With Amberlyte IRA-400; In methanol; water; acetone; for 72h; Ambient temperature;
DOI:10.1016/0008-6215(88)80143-5

Reference yield:

: 117486-50-7,117604-11-2,117604-12-3,117773-05-4
<(1R)-(1,2,4/3,5)-2,3,4-tribenzyloxy-5-benzyloxymethyl-1-cyclohexyl> 2-deoxy-2-(2,4-dinitrophenylamino)-β-D-glucopyranoside triacetate

: 117509-51-0,117604-13-4,117604-14-5,117604-82-7
<(1R)-(1,2,4/3,5)-2,3,4-tribenzyloxy-5-benzyloxymethyl-1-cyclohexyl> 2-acetamido-2-deoxy-β-D-glucopyranoside triacetate

Guidance literature:: With Amberlyte IRA-400; In methanol; water; acetone; for 72h; Ambient temperature;
DOI:10.1016/0008-6215(88)80143-5

Reference yield:

: 64716-98-9,97372-21-9,112419-55-3,116258-19-6
(1SR,2RS,7RS,9SR,10RS)-4,4,12,12-tetramethyl-3,5,11,13-tetraoxatricyclo<8.3.0.0^2,7>tridecan-9-ol

: 117509-51-0,117604-13-4,117604-14-5,117604-82-7
<(1R)-(1,2,4/3,5)-2,3,4-tribenzyloxy-5-benzyloxymethyl-1-cyclohexyl> 2-acetamido-2-deoxy-α-D-glucopyranoside triacetate

Guidance literature:: Multi-step reaction with 6 steps

1: 0.39 g / sodium hydride (50percent) / dimethylformamide / 1 h / Ambient temperature

2: 2.) pyridine / 1.) aq. acetic acid (80percent), 80 deg C, 1 h

3: 1.) sodium methoxide (1M); 2.) sodium hydride (50percent) / 1.) methanol, room temp., 1 h; 2.) N,N-dimethylformamide, room temp., 3 h

4: 75 percent / selenium dioxide, acetic acid / dioxane / 1.5 h / Heating

5: 8.3 percent / calcium sulfate, 2,4,6-trimethylpyridine, silver carbonate, silver perchlorate / CCl₄ / 5 h / Ambient temperature

6: 58 mg / Amberlyte IRA-400 / methanol; acetone; H₂O / 72 h / Ambient temperature

With pyridine; 2,4,6-trimethyl-pyridine; calcium sulfate; selenium(IV) oxide; Amberlyte IRA-400; sodium methylate; silver perchlorate; sodium hydride; acetic acid; silver carbonate; In 1,4-dioxane; methanol; tetrachloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0008-6215(88)80143-5