N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide

Base Information

Chemical Name:N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide
CAS No.:74780-63-5
Molecular Formula:C₂₄H₁₆ClN₃O₆
Molecular Weight:477.861
Hs Code.:

N-phenyl-8-<trans-3-(2-chloro-5-nitrophenyl)-3-oxoprop-1-enyl>-2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide

Synonyms:

Suppliers and Price of N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide

Chemical Property:

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Technology Process of N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide

There total 3 articles about N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 941-69-5
N-phenyl-maleimide

: 74780-52-2
3,11-bis--3,11-diazatricyclo<5.3.1.1^2,6>dodeca-4,8-diene-10,12-dione

: 74780-63-5
N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide

Guidance literature:: With hydroquinone; In tetrahydrofuran; chlorobenzene; at 130 ℃; for 48h;
DOI:10.1039/P19800000362

Reference yield:

: 74780-46-4
trans-1-(2-chloro-5-nitrophenyl)-3-chloroprop-2-en-1-one

: 74780-63-5
N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / tetrahydrofuran / 3 h / 20 °C

2: 87 percent / triethylamine / acetonitrile / 0.17 h

3: 13 percent / hydroquinone / tetrahydrofuran; chlorobenzene / 48 h / 130 °C

With triethylamine; hydroquinone; In tetrahydrofuran; chlorobenzene; acetonitrile;
DOI:10.1039/P19800000362

Reference yield:

: 74780-45-3
1--3-hydroxypyridinium chloride

: 74780-63-5
N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / triethylamine / acetonitrile / 0.17 h

2: 13 percent / hydroquinone / tetrahydrofuran; chlorobenzene / 48 h / 130 °C

With triethylamine; hydroquinone; In tetrahydrofuran; chlorobenzene; acetonitrile;
DOI:10.1039/P19800000362