<2>-<1,12-Bis(triphenylmethylthio)dodecan>--Rotaxan

Base Information

Chemical Name:<2>-<1,12-Bis(triphenylmethylthio)dodecan>--Rotaxan
CAS No.:102435-97-2
Molecular Formula:C₂₈H₅₆*C₅₀H₅₄S₂
Molecular Weight:1111.86
Hs Code.:

<2>-<1,12-Bis(triphenylmethylthio)dodecan>-<Cyclooctacosan>-Rotaxan

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Chemical Property of <2>-<1,12-Bis(triphenylmethylthio)dodecan>--Rotaxan

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Technology Process of <2>-<1,12-Bis(triphenylmethylthio)dodecan>--Rotaxan

There total 3 articles about <2>-<1,12-Bis(triphenylmethylthio)dodecan>--Rotaxan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.8%

: 297-24-5
cyclooctacosane

: 102435-91-6
1,12-Bis(triphenylmethylthio)dodecan

: 102435-97-2
<2>-<1,12-Bis(triphenylmethylthio)dodecan>--Rotaxan

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 130 ℃; for 0.5h;

Reference yield:

: 33528-63-1
dodecane-1,12-dithiol

: 102435-97-2
<2>-<1,12-Bis(triphenylmethylthio)dodecan>--Rotaxan

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / Al₂O₃ / dioxane / 24 h

2: 3.8 percent / p-Me-C₆H₆-SO₃H / toluene / 0.5 h / 130 °C

With aluminum oxide; toluene-4-sulfonic acid; In 1,4-dioxane; toluene;

Reference yield:

: 76-83-5
trityl chloride

: 102435-97-2
<2>-<1,12-Bis(triphenylmethylthio)dodecan>--Rotaxan

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / Al₂O₃ / dioxane / 24 h

2: 3.8 percent / p-Me-C₆H₆-SO₃H / toluene / 0.5 h / 130 °C

With aluminum oxide; toluene-4-sulfonic acid; In 1,4-dioxane; toluene;