dichloro(phenyltelluro)bis(diphenyl telluride)rhodium(III)

Base Information

Chemical Name:dichloro(phenyltelluro)bis(diphenyl telluride)rhodium(III)
CAS No.:74822-05-2
Molecular Formula:C₃₀H₂₅Cl₂RhTe₃
Molecular Weight:942.14
Hs Code.:

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Chemical Property of dichloro(phenyltelluro)bis(diphenyl telluride)rhodium(III)

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Technology Process of dichloro(phenyltelluro)bis(diphenyl telluride)rhodium(III)

There total 1 articles about dichloro(phenyltelluro)bis(diphenyl telluride)rhodium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: rhodium(III) chloride trihydrate

: 1202-36-4
diphenyl telluride

: 74822-05-2
dichloro(phenyltelluro)bis(diphenyl telluride)rhodium(III)

Guidance literature:: With formaldehyd; In ethanol; (Ar); hot soln. of RhCl3*3H2O was added to refluxing soln. of TePh2, after 5 min of refluxing was added 37% aq. CH2O soln. and mixt. was refluxed for further 24 h; ppt. formed on cooling to 0°C was filtered off, washed with hexane and dried; elem. anal.;
DOI:10.1016/S0022-328X(00)83986-8

Reference yield: 52.0%

: 74822-05-2
dichloro(phenyltelluro)bis(diphenyl telluride)rhodium(III)

: 74822-06-3
carbonyldichloro(phenyltelluro)bis(diphenyl telluride)rhodium(III)

Guidance literature:: With carbon monoxide; In benzene; (Ar); CO was bubbled through soln. of Rh complex for 3 ds; solvent was removed in vac. and residue recrystd. from CH2Cl2/hexane; elem. anal.;
DOI:10.1016/S0022-328X(00)83986-8