Technology Process of
There total 1 articles about which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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In
ethanol; di-isopropyl ether;
Irradiation (UV/VIS); a soln. of Mn carbonyl in 4% (by volume) ethanol-diisopropyl ether mixt. irradiating with a 250-W Hg lamp for 15 min under N2; identified by IR spectrum;
- Guidance literature:
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In
decalin;
react. carried out in decalin at 49.9°C in the dark; monitored by IR;
DOI:10.1021/ja00303a011
- Guidance literature:
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In
hexane;
Irradiation (UV/VIS); mercury discharge lamp; 4.0 h; not isolated, monitored by IR;
DOI:10.1039/c39850001287