[(Me₅C₅(-PCH(o-anisyl)O-(cyclic)))W(CO)5]

Base Information

Chemical Name:[(Me₅C₅(-PCH(o-anisyl)O-(cyclic)))W(CO)5]
CAS No.:1215290-20-2
Molecular Formula:C₂₃H₂₃O₇PW
Molecular Weight:626.255
Hs Code.:

[(Me<sub>5</sub>C<sub>5</sub>(-PCH(o-anisyl)O-(cyclic)))W(CO)5]

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Chemical Property of [(Me₅C₅(-PCH(o-anisyl)O-(cyclic)))W(CO)5]

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Technology Process of [(Me₅C₅(-PCH(o-anisyl)O-(cyclic)))W(CO)5]

There total 1 articles about [(Me₅C₅(-PCH(o-anisyl)O-(cyclic)))W(CO)5] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 219555-20-1
pentacarbonyl[chloropentamethyl-2,4-cyclopentadien-1-yl-phosphane]tungsten⁽⁰⁾

: 135-02-4
ortho-anisaldehyde

: 1215290-20-2
[(Me₅C₅(-PCH(o-anisyl)O-(cyclic)))W(CO)5]

Guidance literature:: With lithium diisopropylamide; 12-crown-4; In diethyl ether; (Ar); Schlenk techniques; Et2O soln. of lithium diisopropylamide cooled to -80°C; Et2O soln. of (Me5C5P(H)Cl)W(CO)5, 12-crown-4, o-anisaldehyde added; stirred for 2 h while warmed to -20°C; vac. evapn.; extd. with pentane; washed with pentane at -70°C; elem. anal.;
DOI:10.1002/zaac.200900063