Technology Process of C26H39NO4SSi
There total 13 articles about C26H39NO4SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 11 steps
1: sodium tetrahydroborate / methanol
2: 1H-imidazole
3: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II)
4: n-butyllithium / tetrahydrofuran
5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane
6: diethyl ether
7: sodium hexamethyldisilazane; triethylamine / tetrahydrofuran
8: N-Bromosuccinimide / tetrahydrofuran
9: sodium diformamide / acetonitrile
10: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane
11: 1H-imidazole / N,N-dimethyl-formamide
With
1H-imidazole; sodium tetrahydroborate; N-Bromosuccinimide; n-butyllithium; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); sodium diformamide; sodium hexamethyldisilazane; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 2 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane
2: 1H-imidazole / N,N-dimethyl-formamide
With
1H-imidazole; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 8 steps
1: n-butyllithium / tetrahydrofuran
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane
3: diethyl ether
4: sodium hexamethyldisilazane; triethylamine / tetrahydrofuran
5: N-Bromosuccinimide / tetrahydrofuran
6: sodium diformamide / acetonitrile
7: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane
8: 1H-imidazole / N,N-dimethyl-formamide
With
1H-imidazole; N-Bromosuccinimide; n-butyllithium; sodium diformamide; sodium hexamethyldisilazane; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067