Technology Process of C58H54N8O10S2
There total 7 articles about C58H54N8O10S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; sodium L-ascorbate;
In
tetrahydrofuran; water;
at 20 ℃;
for 72h;
DOI:10.1021/jo402522y
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / dichloromethane / 1 h / 20 °C
2: sodium azide / N,N-dimethyl-formamide / 15 h / 20 °C
3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tetrahydrofuran / 72 h / 20 °C
With
sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; triethylamine;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo402522y
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: iron(III) chloride / dichloromethane; nitromethane / 3 h / 20 °C
2.1: boron tribromide / dichloromethane / 12 h / 0 °C / Inert atmosphere
3.1: camphor-10-sulfonic acid / toluene / 3 h / 100 °C / Inert atmosphere
4.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
4.2: 24.25 h / 0 - 20 °C / Inert atmosphere
5.1: hydrogenchloride / methanol; water; tetrahydrofuran / 12 h / Reflux
6.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tetrahydrofuran / 72 h / 20 °C
With
hydrogenchloride; iron(III) chloride; copper(ll) sulfate pentahydrate; camphor-10-sulfonic acid; boron tribromide; sodium hydride; sodium L-ascorbate;
In
tetrahydrofuran; methanol; nitromethane; dichloromethane; water; toluene;
DOI:10.1021/jo402522y