C₃₄H₅₀O₂Si

Base Information

Chemical Name:C₃₄H₅₀O₂Si
CAS No.:1263532-84-8
Molecular Formula:C₃₄H₅₀O₂Si
Molecular Weight:518.855
Hs Code.:

C<sub>34</sub>H<sub>50</sub>O<sub>2</sub>Si

Synonyms:

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Chemical Property of C₃₄H₅₀O₂Si

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Technology Process of C₃₄H₅₀O₂Si

There total 10 articles about C₃₄H₅₀O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₃₃NO₃Si

: 1263532-84-8
C₃₄H₅₀O₂Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: titanium tetrachloride / toluene / -78 °C / Inert atmosphere

1.2: -78 - -50 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.2: 0.5 h / 0 °C / Inert atmosphere

3.1: lithium borohydride / tetrahydrofuran; diethyl ether / 1 h / 0 °C / Inert atmosphere

4.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

5.1: sodium tetrahydroborate / N,N,N,N,N,N-hexamethylphosphoric triamide / 4 h / 20 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 20 °C / Inert atmosphere

7.1: dmap; triethylamine / dichloromethane / 0 °C / Inert atmosphere

8.1: dmap / dichloromethane / 21 h / Inert atmosphere

With 2,6-dimethylpyridine; dmap; sodium tetrahydroborate; lithium borohydride; tetrabutyl ammonium fluoride; titanium tetrachloride; triethylamine; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; toluene;
DOI:10.1002/anie.201004746

Reference yield:

: C₁₆H₂₅NO₄

: 1263532-84-8
C₃₄H₅₀O₂Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

1.2: 0.5 h / 0 °C / Inert atmosphere

2.1: lithium borohydride / tetrahydrofuran; diethyl ether / 1 h / 0 °C / Inert atmosphere

3.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

4.1: sodium tetrahydroborate / N,N,N,N,N,N-hexamethylphosphoric triamide / 4 h / 20 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 20 °C / Inert atmosphere

6.1: dmap; triethylamine / dichloromethane / 0 °C / Inert atmosphere

7.1: dmap / dichloromethane / 21 h / Inert atmosphere

With 2,6-dimethylpyridine; dmap; sodium tetrahydroborate; lithium borohydride; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane;
DOI:10.1002/anie.201004746

Reference yield:

: C₂₂H₃₉NO₄Si

: 1263532-84-8
C₃₄H₅₀O₂Si

Guidance literature:: Multi-step reaction with 6 steps

1: lithium borohydride / tetrahydrofuran; diethyl ether / 1 h / 0 °C / Inert atmosphere

2: dmap; triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

3: sodium tetrahydroborate / N,N,N,N,N,N-hexamethylphosphoric triamide / 4 h / 20 °C / Inert atmosphere

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 20 °C / Inert atmosphere

5: dmap; triethylamine / dichloromethane / 0 °C / Inert atmosphere

6: dmap / dichloromethane / 21 h / Inert atmosphere

With dmap; sodium tetrahydroborate; lithium borohydride; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane;
DOI:10.1002/anie.201004746