Technology Process of C25H32N2O5
There total 1 articles about C25H32N2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 20 ℃;
Cooling with ice;
DOI:10.1021/jm301630s
- Guidance literature:
-
With
hydrogenchloride; water;
In
ethyl acetate;
at 20 ℃;
for 1h;
DOI:10.1021/jm301630s
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride; water / ethyl acetate / 1 h / 20 °C
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Cooling with ice
3: hydrogen; palladium on activated charcoal / ethyl acetate / 2 h / 760.05 Torr
With
hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; palladium on activated charcoal; water; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; ethyl acetate;
DOI:10.1021/jm301630s