C₁₆H₁₅BrO₄

Base Information

Chemical Name:C₁₆H₁₅BrO₄
CAS No.:1263362-58-8
Molecular Formula:C₁₆H₁₅BrO₄
Molecular Weight:351.197
Hs Code.:

C<sub>16</sub>H<sub>15</sub>BrO<sub>4</sub>

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Suppliers and Price of C₁₆H₁₅BrO₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₅BrO₄

Chemical Property:

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Technology Process of C₁₆H₁₅BrO₄

There total 1 articles about C₁₆H₁₅BrO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 99-76-3,156291-94-0
methyl 4-hydroxylbenzoate

: 1263362-58-8
C₁₆H₁₅BrO₄

Guidance literature:: methyl 4-hydroxylbenzoate; With bromine; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;

Benzyloxymethyl chloride; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jo1022102

Reference yield:

: 1263362-58-8
C₁₆H₁₅BrO₄

: 1263362-61-3
C₁₅H₁₅BrO₃

Guidance literature:: With lithium borohydride; In diethyl ether; at 0 ℃; for 20.5h; Inert atmosphere;
DOI:10.1021/jo1022102

Reference yield:

: 1263362-58-8
C₁₆H₁₅BrO₄

: 1263362-04-4
C₂₆H₃₄O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium borohydride / diethyl ether / 20.5 h / 0 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C / Inert atmosphere

3.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexanes; diethyl ether / 15 h / Inert atmosphere; Cooling

3.2: 0.25 h / Inert atmosphere; Cooling

3.3: 20 °C / Inert atmosphere; Cooling

With lithium borohydride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sodium hydride; In tetrahydrofuran; hexanes; diethyl ether; mineral oil;
DOI:10.1021/jo1022102