S-benzyl-5-didesoxy-5,6-O-isopropylidene-1,2-O-methyl-3-α-D-xylo-hexeno-5-thio-5-furannose

Base Information

Chemical Name:S-benzyl-5-didesoxy-5,6-O-isopropylidene-1,2-O-methyl-3-α-D-xylo-hexeno-5-thio-5-furannose
CAS No.:68397-11-5
Molecular Formula:C₁₇H₂₂O₄S
Molecular Weight:322.425
Hs Code.:

Synonyms:

Suppliers and Price of S-benzyl-5-didesoxy-5,6-O-isopropylidene-1,2-O-methyl-3-α-D-xylo-hexeno-5-thio-5-furannose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-benzyl-5-didesoxy-5,6-O-isopropylidene-1,2-O-methyl-3-α-D-xylo-hexeno-5-thio-5-furannose

Chemical Property:

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Technology Process of S-benzyl-5-didesoxy-5,6-O-isopropylidene-1,2-O-methyl-3-α-D-xylo-hexeno-5-thio-5-furannose

There total 3 articles about S-benzyl-5-didesoxy-5,6-O-isopropylidene-1,2-O-methyl-3-α-D-xylo-hexeno-5-thio-5-furannose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57032-31-2
6-Benzylthio-6-deoxy-1,2-O-isopropyliden-3-O-methyl-α-D-xylo-hexofuranos-5-ulose

: 68397-11-5
S-benzyl-5-didesoxy-5,6-O-isopropylidene-1,2-O-methyl-3-α-D-xylo-hexeno-5-thio-5-furannose

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / ethanol / 3 h / 25 °C

2: NaOMe / bis-(2-methoxy-ethyl) ether / 1.) -15 deg C, 1 h, 2.) 20 deg C, 12 h, 3.) 160 deg C, 30 min

With sodium methylate; In ethanol; diethylene glycol dimethyl ether;
DOI:10.1002/hlca.19800630104

Reference yield:

: 68397-08-0,68397-38-6,74081-53-1
S-benzyl-6-desoxy-5-O-isopropylidene-1,2-O-methyl-3-tosylhydrazono-5-α-D-xylo-thio-6-hexafurannose

: 68397-11-5
S-benzyl-5-didesoxy-5,6-O-isopropylidene-1,2-O-methyl-3-α-D-xylo-hexeno-5-thio-5-furannose

: 68397-12-6
(Z)-S-benzyl-6-didesoxy-5,6-O-isopropylidene-1,2-O-methyl-3-α-D-xylo-hexeno-5-thio-6-furannose

: 68397-13-7
(E)-S-benzyl-6-didesoxy-5,6-O-isopropylidene-1,2-O-methyl-3-α-D-xylo-hexeno-5-thio-6-furannose

: (Z)-S-benzyl-6-didesoxy-5,6-O-isopropylidene-1,2-O-methyl-3-β-L-threo-hexeno-4-thio-6-furannose

Guidance literature:: With sodium methylate; In diethylene glycol dimethyl ether; Yield given. Further byproducts given. Yields of byproduct given; 1.) -15 deg C, 1 h, 2.) 20 deg C, 12 h, 3.) 160 deg C, 30 min;
DOI:10.1002/hlca.19800630104