C₁₅H₁₄Cl₂O

Base Information

Chemical Name:C₁₅H₁₄Cl₂O
CAS No.:1432498-72-0
Molecular Formula:C₁₅H₁₄Cl₂O
Molecular Weight:281.182
Hs Code.:

C<sub>15</sub>H<sub>14</sub>Cl<sub>2</sub>O

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₄Cl₂O

Chemical Property:

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Technology Process of C₁₅H₁₄Cl₂O

There total 9 articles about C₁₅H₁₄Cl₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3917-57-5
N,N-dimethyl-2-(2-methylphenyl)ethanamide

: 1432498-72-0
C₁₅H₁₄Cl₂O

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 20 h / 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / toluene / 4 h / -78 - 0 °C / Inert atmosphere

3.1: zinc dibromide; lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 - -20 °C / Inert atmosphere

3.2: 2 h / -10 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

5.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / -20 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; zinc dibromide; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja4025963

Reference yield:

: C₁₂H₁₅ClO

: 1432498-72-0
C₁₅H₁₄Cl₂O

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridinium chlorochromate / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

2.1: zinc dibromide; lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 - -20 °C / Inert atmosphere

2.2: 2 h / -10 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

4.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / -20 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium hydrogencarbonate; Dess-Martin periodane; pyridinium chlorochromate; zinc dibromide; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja4025963

Reference yield:

: C₁₈H₂₄Cl₂OSi

: 1432498-72-0
C₁₅H₁₄Cl₂O

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

2: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / -20 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja4025963