C₃₄H₃₃N₃O₃

Base Information

Chemical Name:C₃₄H₃₃N₃O₃
CAS No.:1567846-64-3
Molecular Formula:C₃₄H₃₃N₃O₃
Molecular Weight:531.654
Hs Code.:

C<sub>34</sub>H<sub>33</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₃₃N₃O₃

Chemical Property:

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Technology Process of C₃₄H₃₃N₃O₃

There total 11 articles about C₃₄H₃₃N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₄H₃₃N₃O₄

: 1567846-64-3
C₃₄H₃₃N₃O₃

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmcl.2014.01.004

Reference yield:

: 1567846-63-2
C₁₈H₁₅BrN₂O₃

: 1567846-64-3
C₃₄H₃₃N₃O₃

Guidance literature:: Multi-step reaction with 5 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 110 °C

2: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

3: lithium hydroxide; methanol / tetrahydrofuran / Reflux

4: methanol; sodium tetrahydroborate / tetrahydrofuran / 20 °C

5: trifluoroacetic acid; triethylsilane / dichloromethane / 20 °C

With methanol; triethylsilane; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; N,N-dimethyl-formamide; 1: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.01.004

Reference yield:

: 586-76-5
4-Bromobenzoic acid

: 1567846-64-3
C₃₄H₃₃N₃O₃

Guidance literature:: Multi-step reaction with 9 steps

1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

2: n-butyllithium / tetrahydrofuran / -78 - 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C

4: lithium hydroxide; methanol / tetrahydrofuran / 70 °C

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 110 °C

6: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

7: lithium hydroxide; methanol / tetrahydrofuran / Reflux

8: methanol; sodium tetrahydroborate / tetrahydrofuran / 20 °C

9: trifluoroacetic acid; triethylsilane / dichloromethane / 20 °C

With methanol; triethylsilane; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; N,N-dimethyl-formamide; 5: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.01.004