N'-cyclohexylidene-4-methoxybenzohydrazide

Base Information

• Chemical Name: N'-cyclohexylidene-4-methoxybenzohydrazide
• CAS No.: 302910-62-9
• Molecular Formula: C₁₄H₁₈N₂O₂
• Molecular Weight: 246.309
• DSSTox Substance ID: DTXSID90354347
• Mol file: 302910-62-9.mol

Synonyms:N'-cyclohexylidene-4-methoxybenzohydrazide;302910-62-9;DTXSID90354347;STK024591;AKOS000483363

Chemical Property of N'-cyclohexylidene-4-methoxybenzohydrazide

Chemical Property:

• XLogP3: 2.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 246.136827821
• Heavy Atom Count: 18
• Complexity: 299

Purity/Quality:

N'-cyclohexylidene-4-methoxybenzohydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)C(=O)NN=C2CCCCC2

Technology Process of N'-cyclohexylidene-4-methoxybenzohydrazide

There total 1 articles about N'-cyclohexylidene-4-methoxybenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + 4-methoxybenzoic acid hydrazide (3290-99-1) → N-cyclohexylidene-4-methoxybenzohydrazide (302910-62-9)

Guidance literature:

Reflux;

DOI:10.1007/s11172-010-0094-3

Reference yield: 85.0%

N-cyclohexylidene-4-methoxybenzohydrazide (302910-62-9) + phosphonic acid diethyl ester (762-04-9) → diethyl {1-[2-(4-methoxybenzoyl)hydrazino]cyclohexyl}phosphonate (1260116-82-2)

Guidance literature:

With [tetra(tert-butyl)phthalocyanine]aluminum chloride; at 80 ℃; for 4h; Inert atmosphere;

DOI:10.1007/s11172-010-0094-3

upstream raw materials:

cyclohexanone

4-methoxybenzoic acid hydrazide

Downstream raw materials:

diethyl {1-[2-(4-methoxybenzoyl)hydrazino]cyclohexyl}phosphonate