((C₆H₅)3Ge)3GeI

Base Information

Chemical Name:((C₆H₅)3Ge)3GeI
CAS No.:1265901-87-8
Molecular Formula:C₅₄H₄₅Ge₄I
Molecular Weight:1111.22
Hs Code.:

Synonyms:

Suppliers and Price of ((C₆H₅)3Ge)3GeI

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ((C₆H₅)3Ge)3GeI

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ((C₆H₅)3Ge)3GeI

There total 2 articles about ((C₆H₅)3Ge)3GeI which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 2816-38-8
(Ph₃Ge)3GeH

: 75-11-6
diiodomethane

: 1265901-87-8
((C₆H₅)3Ge)3GeI

Guidance literature:: With [Ph₃C]PF₆; In further solvent(s); byproducts: Ph3CH, [CH2I][PF6]; (N2); Schlenk technique; mixt. of Ge compd. and Ph3CPF6 in CH2I2 was heated with stirring at 90°C for 24 h; filtered through Celite; evapd. (vac.); washed (hexane); dried (vac.); recrystd. (C6H6); elem. anal.;
DOI:10.1021/om101091c

Reference yield:

: 1265901-88-9
(Ph₃Ge)3GeNMe₂

: 1265901-87-8
((C₆H₅)3Ge)3GeI

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile

2: [Ph₃C]PF₆ / further solvent(s)

With [Ph₃C]PF₆; In acetonitrile;
DOI:10.1021/om101091c