Technology Process of C25H30O6
There total 5 articles about C25H30O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: di(n-butyl)tin oxide / toluene / 2 h / 110 °C
1.2: 14 h / 65 °C
2.1: pyridine; dmap / 5 h / 20 °C
With
pyridine; dmap; di(n-butyl)tin oxide;
In
toluene;
DOI:10.1021/ol501095w
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride; 1H-imidazole / N,N-dimethyl-formamide / 0.25 h / 0 - 20 °C
1.2: 14 h / 20 °C
2.1: bismuth(III) chloride; water / acetonitrile / 14 h / 20 °C
3.1: di(n-butyl)tin oxide / toluene / 2 h / 110 °C
3.2: 14 h / 65 °C
4.1: pyridine; dmap / 5 h / 20 °C
With
pyridine; 1H-imidazole; dmap; bismuth(III) chloride; water; sodium hydride; di(n-butyl)tin oxide;
In
N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/ol501095w
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: toluene-4-sulfonic acid / 0.17 h / 20 °C
2.1: sodium hydride; 1H-imidazole / N,N-dimethyl-formamide / 0.25 h / 0 - 20 °C
2.2: 14 h / 20 °C
3.1: bismuth(III) chloride; water / acetonitrile / 14 h / 20 °C
4.1: di(n-butyl)tin oxide / toluene / 2 h / 110 °C
4.2: 14 h / 65 °C
5.1: pyridine; dmap / 5 h / 20 °C
With
pyridine; 1H-imidazole; dmap; bismuth(III) chloride; water; sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid;
In
N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/ol501095w