Phthalimide, N,N'-azodi-

Base Information

• Chemical Name: Phthalimide, N,N'-azodi-
• CAS No.: 24965-34-2
• Molecular Formula: C₁₆H₈N₄O₄
• Molecular Weight: 320.264
• NSC Number: 354297
• DSSTox Substance ID: DTXSID20418648
• Wikidata: Q82229264
• Mol file: 24965-34-2.mol

Synonyms:NSC354297;24965-34-2;Phthalimide, N,N'-azodi-;DTXSID20418648;ZTHBQCBCHJPWRS-ISLYRVAYSA-N;NSC-354297;Isoindole-1,3(2H,3H)-dione, 2,2'-azobis-

Chemical Property of Phthalimide, N,N'-azodi-

Chemical Property:

• XLogP3: 2.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 2
• Exact Mass: 320.05455475
• Heavy Atom Count: 24
• Complexity: 544

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C(=O)N(C2=O)N=NN3C(=O)C4=CC=CC=C4C3=O
• Isomeric SMILES: C1=CC=C2C(=C1)C(=O)N(C2=O)/N=N/N3C(=O)C4=CC=CC=C4C3=O

Technology Process of Phthalimide, N,N'-azodi-

There total 1 articles about Phthalimide, N,N'-azodi- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

N-aminophthalamide (1875-48-5) + 5-phenylspiro(1-pyrazoline-3,1'-cyclopropane) (252921-91-8) → 1,4-bis-phthaloyltetrazene (24965-34-2) + [2,2'-biisoindoline]-1,1',3,3'-tetraone (4388-29-8) + N-{3-phenylspiro[1-pyrazolinio-5,1'-cyclopropane]}-N-phthalimidoamide + N-{5-phenylspiro[1-pyrazolinio-3,1'-cyclopropane]}-N-phthalimidoamide

Guidance literature:

With lead(IV) acetate; potassium carbonate; In dichloromethane; at -30 - -20 ℃; for 1.5h; Further byproducts given;

DOI:10.1007/BF02495296

upstream raw materials:

N-aminophthalamide

5-phenylspiro(1-pyrazoline-3,1'-cyclopropane)