Diisopropyl (phenylsulfonyl)phosphoramidate

Base Information

• Chemical Name: Diisopropyl (phenylsulfonyl)phosphoramidate
• CAS No.: 33215-71-3
• Molecular Formula: C₂₄H₂₉N₂O₇PS₂
• Molecular Weight: 552.609

Synonyms:

Chemical Property of Diisopropyl (phenylsulfonyl)phosphoramidate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Diisopropyl (phenylsulfonyl)phosphoramidate

There total 3 articles about Diisopropyl (phenylsulfonyl)phosphoramidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

diisopropyl trimethylsily phosphite (24350-54-7) + (E)-N,N′-(cyclohexa-2,5-diene-1,4-diylidene)dibenzenesulfonamide (1050-82-4,43134-47-0,43134-48-1) → Diisopropyl (phenylsulfonyl)phosphoramidate (33215-71-3,114579-83-8,114580-47-1)

Guidance literature:

at 110 - 120 ℃; for 0.166667h;

Reference yield:

diisopropyl trimethylsily phosphite (24350-54-7) + N,N'-bis(phenylsulfonyl)-p-benzoquinone diimine (1050-82-4,43134-47-0,43134-48-1) → Diisopropyl (phenylsulfonyl)phosphoramidate (33215-71-3,114579-83-8,114580-47-1)

Guidance literature:

With butan-1-ol; Multistep reaction;

Reference yield:

→ Diisopropyl (phenylsulfonyl)phosphoramidate (33215-71-3,114579-83-8,114580-47-1)

Guidance literature:

Chinondisulfonimid 1a, Triisopropylphosphit;

DOI:10.1016/S0040-4039(01)96740-1

upstream raw materials:

diisopropyl trimethylsily phosphite

(E)-N,N′-(cyclohexa-2,5-diene-1,4-diylidene)dibenzenesulfonamide

N,N'-bis(phenylsulfonyl)-p-benzoquinone diimine

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