2-Nitro-3,4,5-trimethyl-phenyl-acetaldoxim

Base Information

Chemical Name:2-Nitro-3,4,5-trimethyl-phenyl-acetaldoxim
CAS No.:103565-14-6
Molecular Formula:C₁₁H₁₄N₂O₃
Molecular Weight:222.244
Hs Code.:

Synonyms:

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Chemical Property of 2-Nitro-3,4,5-trimethyl-phenyl-acetaldoxim

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Technology Process of 2-Nitro-3,4,5-trimethyl-phenyl-acetaldoxim

There total 6 articles about 2-Nitro-3,4,5-trimethyl-phenyl-acetaldoxim which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100061-17-4
3,4,5-Trimethyl-2,β-dinitro-styrol

: 103565-14-6
2-Nitro-3,4,5-trimethyl-phenyl-acetaldoxim

Guidance literature:: With hydrogen; acetic acid; palladium on activated charcoal;
DOI:10.1021/jo01079a020

Reference yield:

: 1076-88-6
3,4,5-trimethylbenzoic acid

: 103565-14-6
2-Nitro-3,4,5-trimethyl-phenyl-acetaldoxim

Guidance literature:: Multi-step reaction with 5 steps

1: SOCl₂

2: H₂ / Pd-BaSO₄

3: KNO₃, H₂SO₄

4: (i) aq. KOH, (ii) NaOAc, Ac₂O

5: H₂, AcOH / Pd-C

With thionyl chloride; sulfuric acid; hydrogen; acetic acid; potassium nitrate; palladium on activated charcoal; palladium on barium sulfate;
DOI:10.1021/jo01079a020

Reference yield:

: 2047-21-4
3,4,5-trimethylacetophenone

: 103565-14-6
2-Nitro-3,4,5-trimethyl-phenyl-acetaldoxim

Guidance literature:: Multi-step reaction with 6 steps

1: aq. NaOBr

2: SOCl₂

3: H₂ / Pd-BaSO₄

4: KNO₃, H₂SO₄

5: (i) aq. KOH, (ii) NaOAc, Ac₂O

6: H₂, AcOH / Pd-C

With thionyl chloride; sodium hypobromide; sulfuric acid; hydrogen; acetic acid; potassium nitrate; palladium on activated charcoal; palladium on barium sulfate;
DOI:10.1021/jo01079a020