(2-t-butylphenylphosphinoethyl)di-t-butylphenylstannane

Base Information

Chemical Name:(2-t-butylphenylphosphinoethyl)di-t-butylphenylstannane
CAS No.:84668-50-8
Molecular Formula:C₂₆H₄₁PSn
Molecular Weight:503.295
Hs Code.:

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Chemical Property of (2-t-butylphenylphosphinoethyl)di-t-butylphenylstannane

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Technology Process of (2-t-butylphenylphosphinoethyl)di-t-butylphenylstannane

There total 2 articles about (2-t-butylphenylphosphinoethyl)di-t-butylphenylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30191-23-2
phenyldi(tert-butyl)tin chloride

: 84668-50-8
(2-t-butylphenylphosphinoethyl)di-t-butylphenylstannane

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether

2: AIBN / neat (no solvent)

With LiAlH₄; AIBN; In diethyl ether;
DOI:10.1016/S0022-328X(00)83797-3

Reference yield:

: 84668-48-4
di-t-butylphenyltin hydride

: 84668-89-3
t-butyl-phenyl-vinylphosphine

: 84668-50-8
(2-t-butylphenylphosphinoethyl)di-t-butylphenylstannane

Guidance literature:: With AIBN; In neat (no solvent); (N2 or Ar); educts mixt. in molar ratio 1/1 warmed slowly to 70°C for 8-15 h with stepwise addn. of AIBN; distd. (vac.); elem. anal.;
DOI:10.1016/S0022-328X(00)83797-3

Reference yield: 72.0%

: 84668-50-8
(2-t-butylphenylphosphinoethyl)di-t-butylphenylstannane

: 84668-47-3
((CH₃)3C)2(C₆H₅)Sn(CH₂)2P(O)(C₆H₅)C(CH₃)3

Guidance literature:: With KMnO₄; In acetone; byproducts: MnO2; (N2 or Ar); satd. soln. of KMnO4 added dropwise to educt in acetone; filtered, filtrate distd.; elem. anal.;
DOI:10.1016/S0022-328X(00)83797-3