Pt(OCOC₆H₅)2(P(C₆H₅)3)2

Base Information

Chemical Name:Pt(OCOC₆H₅)2(P(C₆H₅)3)2
CAS No.:20555-32-2
Molecular Formula:C₅₀H₄₀O₄P₂Pt
Molecular Weight:961.893
Hs Code.:

Pt(OCOC<sub>6</sub>H<sub>5</sub>)2(P(C<sub>6</sub>H<sub>5</sub>)3)2

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Chemical Property of Pt(OCOC₆H₅)2(P(C₆H₅)3)2

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Technology Process of Pt(OCOC₆H₅)2(P(C₆H₅)3)2

There total 2 articles about Pt(OCOC₆H₅)2(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 14221-02-4
tetrakis(triphenylphosphine)platinum

: 644-31-5
acetyl benzoyl peroxide

: 20555-32-2,34445-04-0
Pt(OCOC₆H₅)2(P(C₆H₅)3)2

Guidance literature:: In benzene; soln. of peroxide added to soln. of Pt complex, stirred at room temp. for 30 min, under N2; concd., pptd. with light petroleum, recrystd. from CH2Cl2-light petroleum, dried in vac.; elem. anal.;

Reference yield: 66.0%

: 614-45-9
tert-Butyl peroxybenzoate

: 14221-02-4
tetrakis(triphenylphosphine)platinum

: 20555-32-2,34445-04-0
Pt(OCOC₆H₅)2(P(C₆H₅)3)2

Guidance literature:: In dichloromethane; soln. of benzoate added to soln. of Pt complex, under N2; pptd. with MeOH;

Reference yield: 69.8%

: 1830-54-2
3-oxopentanedioic acid dimethyl ester

: 20555-32-2,34445-04-0
Pt(OCOC₆H₅)2(P(C₆H₅)3)2

: [1,3-bis(methoxycarbonyl)-2-oxopropane-1,3-diyl]bis(triphenylphosphine)platinum

Guidance literature:: In ethanol; a susp. of Pt complex and dialkyl 3-oxopentanedioate in EtOH heating under reflux for 1 h, filtering, evapg., dissolving in CH2Cl2, Et2O adding, white solid sepg. off; purified by recrystallization from CH2Cl2-light petroleum; identified by elem. anal., IR, NMR spectra and single crystal X-ray diffraction;
DOI:10.1039/DT9840001993