(1S,2R)-((E)-2-Hex-1-enyl)-cyclopropanecarbaldehyde

Base Information

Chemical Name:(1S,2R)-((E)-2-Hex-1-enyl)-cyclopropanecarbaldehyde
CAS No.:98393-16-9
Molecular Formula:C₁₀H₁₆O
Molecular Weight:152.236
Hs Code.:

Synonyms:

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Chemical Property of (1S,2R)-((E)-2-Hex-1-enyl)-cyclopropanecarbaldehyde

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Technology Process of (1S,2R)-((E)-2-Hex-1-enyl)-cyclopropanecarbaldehyde

There total 12 articles about (1S,2R)-((E)-2-Hex-1-enyl)-cyclopropanecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51703-66-3
(S)-(-)-1-heptyn-3-ol

: 98393-16-9
(1S,2R)-((E)-2-Hex-1-enyl)-cyclopropanecarbaldehyde

Guidance literature:: Multi-step reaction with 9 steps

1: imidazole / dimethylformamide / 25 °C

2: EtMgBr / dimethylformamide / 2 h / Ambient temperature

3: DMAP, NEt₃ / CH₂Cl₂ / 0.33 h / Ambient temperature

4: (Bu)4N⁽¹⁺⁾*F^(1-) / tetrahydrofuran / 1.25 h / Ambient temperature

5: H₂ / Pd/Lindlar / methanol

6: DBU, 5percent Pd(dppe)2 / tetrahydrofuran / 1.25 h / 25 °C

8: 80 percent / Pd(dppe)2

With 1H-imidazole; dmap; bis[1,2-bis(diphenylphosphino)ethane]palladium⁽⁰⁾; ethylmagnesium bromide; tetrabutyl ammonium fluoride; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; Lindlar's catalyst; bis[1,2-bis(diphenylphosphino)ethane]palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)94910-4

Reference yield:

: 90246-28-9
(-)-(S)-1-(trimethylsilyl)hept-1-yn-3-ol

: 98393-16-9
(1S,2R)-((E)-2-Hex-1-enyl)-cyclopropanecarbaldehyde

Guidance literature:: Multi-step reaction with 10 steps

1: tetrabutylammonium fluoride / tetrahydrofuran / 1 h / Ambient temperature

2: imidazole / dimethylformamide / 25 °C

3: EtMgBr / dimethylformamide / 2 h / Ambient temperature

4: DMAP, NEt₃ / CH₂Cl₂ / 0.33 h / Ambient temperature

5: (Bu)4N⁽¹⁺⁾*F^(1-) / tetrahydrofuran / 1.25 h / Ambient temperature

6: H₂ / Pd/Lindlar / methanol

7: DBU, 5percent Pd(dppe)2 / tetrahydrofuran / 1.25 h / 25 °C

9: 80 percent / Pd(dppe)2

With 1H-imidazole; dmap; bis[1,2-bis(diphenylphosphino)ethane]palladium⁽⁰⁾; ethylmagnesium bromide; tetrabutyl ammonium fluoride; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; Lindlar's catalyst; bis[1,2-bis(diphenylphosphino)ethane]palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)94910-4

Reference yield:

: 503088-35-5
tert-Butyl-((S)-1-ethynyl-pentyloxy)-dimethyl-silane

: 98393-16-9
(1S,2R)-((E)-2-Hex-1-enyl)-cyclopropanecarbaldehyde

Guidance literature:: Multi-step reaction with 8 steps

1: EtMgBr / dimethylformamide / 2 h / Ambient temperature

2: DMAP, NEt₃ / CH₂Cl₂ / 0.33 h / Ambient temperature

3: (Bu)4N⁽¹⁺⁾*F^(1-) / tetrahydrofuran / 1.25 h / Ambient temperature

4: H₂ / Pd/Lindlar / methanol

5: DBU, 5percent Pd(dppe)2 / tetrahydrofuran / 1.25 h / 25 °C

7: 80 percent / Pd(dppe)2

With dmap; bis[1,2-bis(diphenylphosphino)ethane]palladium⁽⁰⁾; ethylmagnesium bromide; tetrabutyl ammonium fluoride; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; Lindlar's catalyst; bis[1,2-bis(diphenylphosphino)ethane]palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)94910-4