benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-carbamoyl-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate

Base Information

Chemical Name:benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-carbamoyl-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate
CAS No.:137845-76-2
Molecular Formula:C₃₃H₃₈N₄O₁₀
Molecular Weight:650.686
Hs Code.:

benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-carbamoyl-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate

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Chemical Property of benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-carbamoyl-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate

Chemical Property:

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Technology Process of benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-carbamoyl-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate

There total 5 articles about benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-carbamoyl-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(S,R)-carbamoyl-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-6'-(pyridylthio)-β-D-ribo-1',4'-decafuranuronate

: 137845-76-2,137845-77-3
benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-carbamoyl-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate

Guidance literature:: With azobisisobutyronitrile; tri-n-butyl-tin hydride; In benzene; for 3h; Yield given; Heating;
DOI:10.1021/jm00079a007

Reference yield:

: 135056-68-7
(S)-2-Benzyloxycarbonylamino-5-carbamoyl-hex-5-enoic acid benzyl ester

: 137845-76-2,137845-77-3
benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-carbamoyl-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0.25 h / 0 °C / Irradiation

2: Bu3SnH, α,α'-azoisobutyronitrile (AIBN) / benzene / 3 h / Heating

With azobisisobutyronitrile; tri-n-butyl-tin hydride; In tetrahydrofuran; benzene;
DOI:10.1021/jm00079a007

Reference yield:

: C₁₇H₂₂N₂O₉

: 137845-76-2,137845-77-3
benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-carbamoyl-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 1 h / 0 °C

2: tetrahydrofuran / 0.25 h / 0 °C / Irradiation

3: Bu3SnH, α,α'-azoisobutyronitrile (AIBN) / benzene / 3 h / Heating

With azobisisobutyronitrile; tri-n-butyl-tin hydride; In tetrahydrofuran; benzene;
DOI:10.1021/jm00079a007