bis[1,2-bis(diphenylphosphino)ethane]carbonylruthenium

Base Information

Chemical Name:bis[1,2-bis(diphenylphosphino)ethane]carbonylruthenium
CAS No.:83111-23-3
Molecular Formula:C₅₃H₄₈OP₄Ru
Molecular Weight:925.929
Hs Code.:

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Chemical Property of bis[1,2-bis(diphenylphosphino)ethane]carbonylruthenium

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Technology Process of bis[1,2-bis(diphenylphosphino)ethane]carbonylruthenium

There total 2 articles about bis[1,2-bis(diphenylphosphino)ethane]carbonylruthenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: bis[bis(diphenylphosphino)ethane-P,P'](styrene)ruthenium

: 83111-23-3
bis[1,2-bis(diphenylphosphino)ethane]carbonylruthenium

Guidance literature:: With carbon monoxide; In toluene; CO bubbling through a soln. of the complex for 2 h at room temp., filtering, concg., light petroleum adding, cooling to -20°C, after 24 h yellow-orange crystals collecting, washing with light petroleum and drying in vacuo; identified by elem. anal., IR and NMR spectra;

Reference yield:

: 83083-02-7
Ru(C₆H₄CH₃)(O₂CH)(CO)(P(C₆H₅)3)2

: 83111-23-3
bis[1,2-bis(diphenylphosphino)ethane]carbonylruthenium

Guidance literature:: With bis-(diphenylphosphino)-ethane; In not given; decarboxylation of educt in presence of dppe;
DOI:10.1016/S0022-328X(00)85709-5