Technology Process of C24H25NO2Si
There total 3 articles about C24H25NO2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C28H36N2O2Si;
With
lithium diisopropyl amide;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 1h;
With
hydrogenchloride;
In
ethanol;
at 80 ℃;
for 16h;
DOI:10.3987/COM-12-S(N)131
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride / water / 20 °C / pH < 5
2.1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 16 h / 90 °C
3.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / 0 - 20 °C
3.2: 16 h / 80 °C
With
hydrogenchloride; tetrakis(triphenylphosphine) palladium(0); sodium carbonate; lithium diisopropyl amide;
In
tetrahydrofuran; 1,2-dimethoxyethane; water;
2.1: |Suzuki-Miyaura Coupling / 3.1: |Fries Phenol Ester Rearrangement;
DOI:10.3987/COM-12-S(N)131
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 16 h / 90 °C
2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / 0 - 20 °C
2.2: 16 h / 80 °C
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate; lithium diisopropyl amide;
In
tetrahydrofuran; 1,2-dimethoxyethane; water;
1.1: |Suzuki-Miyaura Coupling / 2.1: |Fries Phenol Ester Rearrangement;
DOI:10.3987/COM-12-S(N)131
