L-Alanine, N-[2-methyl-N-[N-[2-methyl-N-[1-[(phenylmethoxy)carbonyl]-L-prolyl]alan yl]-L-alanyl]alanyl]-, methyl ester

Base Information

Chemical Name:L-Alanine, N-[2-methyl-N-[N-[2-methyl-N-[1-[(phenylmethoxy)carbonyl]-L-prolyl]alan yl]-L-alanyl]alanyl]-, methyl ester
CAS No.:105590-92-9
Molecular Formula:C₂₈H₄₁N₅O₈
Molecular Weight:575.662
Hs Code.:
Mol file:105590-92-9.mol

Synonyms:

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Chemical Property of L-Alanine, N-[2-methyl-N-[N-[2-methyl-N-[1-[(phenylmethoxy)carbonyl]-L-prolyl]alan yl]-L-alanyl]alanyl]-, methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of L-Alanine, N-[2-methyl-N-[N-[2-methyl-N-[1-[(phenylmethoxy)carbonyl]-L-prolyl]alan yl]-L-alanyl]alanyl]-, methyl ester

There total 3 articles about L-Alanine, N-[2-methyl-N-[N-[2-methyl-N-[1-[(phenylmethoxy)carbonyl]-L-prolyl]alan yl]-L-alanyl]alanyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109772-32-9
N-phenylmethoxycarbonyl-L-alanyl-2-methylalanine

: 105590-92-9
(S)-2-(1-{(S)-1-[1-((S)-1-Methoxycarbonyl-ethylcarbamoyl)-1-methyl-ethylcarbamoyl]-ethylcarbamoyl}-1-methyl-ethylcarbamoyl)-pyrrolidine-1-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline (EEDQ) / toluene / 42 h / 45 °C

2: 83 percent / H₂ / 5percent Pd/C / methanol / 48 h / 18 °C / 53200 Torr

3: 1-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline (EEDQ) / tetrahydrofuran / 72 h / 20 °C

With hydrogen; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; palladium on activated charcoal; In tetrahydrofuran; methanol; toluene;

Reference yield:

: 69305-31-3
methyl N-phenylmethoxycarbonyl-L-alanyl-2-methylalanyl-L-alaninate

: 105590-92-9
(S)-2-(1-{(S)-1-[1-((S)-1-Methoxycarbonyl-ethylcarbamoyl)-1-methyl-ethylcarbamoyl]-ethylcarbamoyl}-1-methyl-ethylcarbamoyl)-pyrrolidine-1-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / H₂ / 5percent Pd/C / methanol / 48 h / 18 °C / 53200 Torr

2: 1-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline (EEDQ) / tetrahydrofuran / 72 h / 20 °C

With hydrogen; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; palladium on activated charcoal; In tetrahydrofuran; methanol;

Reference yield:

: 1148-11-4
N-Benzyloxycarbonyl-L-proline

: 105590-92-9
(S)-2-(1-{(S)-1-[1-((S)-1-Methoxycarbonyl-ethylcarbamoyl)-1-methyl-ethylcarbamoyl]-ethylcarbamoyl}-1-methyl-ethylcarbamoyl)-pyrrolidine-1-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / 1-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline (EEDQ) / toluene / 72 h / 55 °C

2: 1-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline (EEDQ) / tetrahydrofuran / 72 h / 20 °C

With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In tetrahydrofuran; toluene;