4-(6-amino-hexyl)-aniline

Base Information

• Chemical Name: 4-(6-amino-hexyl)-aniline
• CAS No.: 100525-46-0
• Molecular Formula: C₁₂H₂₀N₂
• Molecular Weight: 192.304
• Mol file: 100525-46-0.mol

Synonyms:

Chemical Property of 4-(6-amino-hexyl)-aniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(6-amino-hexyl)-aniline

There total 3 articles about 4-(6-amino-hexyl)-aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-(p-nitrophenyl)hexanenitrile (100134-89-2) → 4-(6-amino-hexyl)-aniline (100525-46-0)

Guidance literature:

With methanol; platinum; at 35 ℃; under 3677.5 Torr; Hydrogenation_.anschliessendes Hydrieren an Raney-Nickel in methanol.NH₃ bei 55-70grad/40-60 at;

DOI:10.1039/jr9570002706

Reference yield:

6-(4-nitrophenyl)-hexanoic acid (65596-92-1) → 4-(6-amino-hexyl)-aniline (100525-46-0)

Guidance literature:

Multi-step reaction with 3 steps

1: PCl₅; aqueous NH₃

2: SOCl₂

3: platinum; methanol / 35 °C / 3677.5 Torr / Hydrogenation_.anschliessendes Hydrieren an Raney-Nickel in methanol.NH₃ bei 55-70grad/40-60 at

With methanol; ammonium hydroxide; thionyl chloride; phosphorus pentachloride; platinum;

DOI:10.1039/jr9570002706

Reference yield:

6-(4-nitro-phenyl)-hexanoic acid amide (66148-02-5) → 4-(6-amino-hexyl)-aniline (100525-46-0)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂

2: platinum; methanol / 35 °C / 3677.5 Torr / Hydrogenation_.anschliessendes Hydrieren an Raney-Nickel in methanol.NH₃ bei 55-70grad/40-60 at

With methanol; thionyl chloride; platinum;

DOI:10.1039/jr9570002706

upstream raw materials:

6-(p-nitrophenyl)hexanenitrile

6-(4-nitrophenyl)-hexanoic acid

6-(4-nitro-phenyl)-hexanoic acid amide

Downstream raw materials:

tri-N-methyl-4-(6-trimethylammonio-hexyl)-anilinium; diiodide