[(bis(N,N'-bis(2,6-diisopropylphenyl)acetamidinate)ZnCl(THF)]

Base Information

Chemical Name:[(bis(N,N'-bis(2,6-diisopropylphenyl)acetamidinate)ZnCl(THF)]
CAS No.:959419-17-1
Molecular Formula:C₃₃H₅₁ClN₂OZn
Molecular Weight:592.624
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Chemical Property of [(bis(N,N'-bis(2,6-diisopropylphenyl)acetamidinate)ZnCl(THF)]

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Technology Process of [(bis(N,N'-bis(2,6-diisopropylphenyl)acetamidinate)ZnCl(THF)]

There total 1 articles about [(bis(N,N'-bis(2,6-diisopropylphenyl)acetamidinate)ZnCl(THF)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: lithium N,N'-bis(2,6-di-isopropylphenyl)tert-butylamidinate

: 7646-85-7,24359-56-6
zinc(II) chloride

: 959419-17-1
[(bis(N,N'-bis(2,6-diisopropylphenyl)acetamidinate)ZnCl(THF)]

Guidance literature:: In tetrahydrofuran; (N2, Schlenk or glove box) a soln. of Li-acetamidine in THF was added dropwise to a soln. of ZnCl2 in THF cooled to -78°C, the mixt. was stirred for 18 h while warming to room temp.; filtered, the solvent was removed under reduced pressure;
DOI:10.1021/ic701061q