P¹,P²-bis(benzyl 5α-androstan-3β-yl) pyrophosphate

Base Information

Chemical Name:P¹,P²-bis(benzyl 5α-androstan-3β-yl) pyrophosphate
CAS No.:230630-67-8
Molecular Formula:C₅₂H₇₆O₇P₂
Molecular Weight:875.119
Hs Code.:

P<sup>1</sup>,P<sup>2</sup>-bis(benzyl 5α-androstan-3β-yl) pyrophosphate

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Chemical Property of P¹,P²-bis(benzyl 5α-androstan-3β-yl) pyrophosphate

Chemical Property:

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Technology Process of P¹,P²-bis(benzyl 5α-androstan-3β-yl) pyrophosphate

There total 4 articles about P¹,P²-bis(benzyl 5α-androstan-3β-yl) pyrophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 230630-64-5
benzyl hydrogen 5α-androstan-3β-yl phosphate

: 230630-67-8
P¹,P²-bis(benzyl 5α-androstan-3β-yl) pyrophosphate

Guidance literature:: With dicyclohexyl-carbodiimide; In benzene; at 20 ℃; for 24h;
DOI:10.1016/S0040-4020(99)00193-3

Reference yield:

: 1224-93-7,7657-50-3,7753-89-1,10085-14-0,15360-52-8,15360-53-9,36216-01-0,36216-02-1,1224-92-6
5α-androstan-3β-ol

: 230630-67-8
P¹,P²-bis(benzyl 5α-androstan-3β-yl) pyrophosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / lithium diisopropylamide / hexane; tetrahydrofuran / 25 h / -78 - 20 °C

2: 96 percent / sodium iodide / acetone / 18 h / Heating

3: dicyclohexyl carbodiimide / benzene / 24 h / 20 °C

With dicyclohexyl-carbodiimide; sodium iodide; lithium diisopropyl amide; In tetrahydrofuran; hexane; acetone; benzene; 1: Esterification / 2: debenzylation / 3: Dehydration;
DOI:10.1016/S0040-4020(99)00193-3

Reference yield:

: 990-91-0
dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate

: 230630-67-8
P¹,P²-bis(benzyl 5α-androstan-3β-yl) pyrophosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / lithium diisopropylamide / hexane; tetrahydrofuran / 25 h / -78 - 20 °C

2: 96 percent / sodium iodide / acetone / 18 h / Heating

3: dicyclohexyl carbodiimide / benzene / 24 h / 20 °C

With dicyclohexyl-carbodiimide; sodium iodide; lithium diisopropyl amide; In tetrahydrofuran; hexane; acetone; benzene; 1: Esterification / 2: debenzylation / 3: Dehydration;
DOI:10.1016/S0040-4020(99)00193-3