Technology Process of 3-(2-hydroxyphenylsulfanyl)-1-(5-cyclohexylpentyl)quinolin-1-ium iodide
There total 3 articles about 3-(2-hydroxyphenylsulfanyl)-1-(5-cyclohexylpentyl)quinolin-1-ium iodide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper(l) iodide; potassium carbonate; ethylene glycol / isopropyl alcohol / 30 h / 80 °C / Inert atmosphere
2: pyridine hydrochloride / 6 h / 220 °C
3: sulfolane / 110 °C
With
copper(l) iodide; pyridine hydrochloride; potassium carbonate; ethylene glycol;
In
sulfolane; isopropyl alcohol;
DOI:10.1016/j.ejmech.2011.02.034
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper(l) iodide; sodium iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 48 h / 110 °C / Inert atmosphere
2: copper(l) iodide; potassium carbonate; ethylene glycol / isopropyl alcohol / 30 h / 80 °C / Inert atmosphere
3: pyridine hydrochloride / 6 h / 220 °C
4: sulfolane / 110 °C
With
copper(l) iodide; pyridine hydrochloride; potassium carbonate; ethylene glycol; sodium iodide; N,N`-dimethylethylenediamine;
In
1,4-dioxane; sulfolane; isopropyl alcohol;
DOI:10.1016/j.ejmech.2011.02.034
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine hydrochloride / 6 h / 220 °C
2: sulfolane / 110 °C
With
pyridine hydrochloride;
In
sulfolane;
DOI:10.1016/j.ejmech.2011.02.034
