{HC{Si(CH₃)2NC₆H₄CH₃}3TiBr}

Base Information

• Chemical Name: {HC{Si(CH₃)2NC₆H₄CH₃}3TiBr}
• CAS No.: 156053-53-1
• Molecular Formula: C₂₈H₄₀BrN₃Si₃Ti
• Molecular Weight: 630.686

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Chemical Property of {HC{Si(CH₃)2NC₆H₄CH₃}3TiBr}

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Technology Process of {HC{Si(CH₃)2NC₆H₄CH₃}3TiBr}

There total 1 articles about {HC{Si(CH₃)2NC₆H₄CH₃}3TiBr} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

TiBr4(THF)2 (60864-10-0) + HC[SiMe2N(4-MeC6H4)]3Li3 → {HC{Si(CH3)2NC6H4CH3}3TiBr} (156053-53-1)

Guidance literature:

In diethyl ether; hexane; pentane; solid TiBr4(THF)2 is added at -50°C to a soln. of the Li-amide (prepared from the appropiate amine and n-BuLi in pentane/ether/hexane at -50°C, stirring for 2 h at room temp.), the mixture is warmed to room temp. over 20 h; the solvent is evapd. in vac., the residue is extd., the extract is concd., cooled to -40°C, elem. anal.;

Reference yield: 73.0%

K{Ru(η5-C5H5)(CO)2} + {HC{Si(CH3)2NC6H4CH3}3TiBr} (156053-53-1) → {HC{Si(CH3)2NC6H4CH3}3Ti(Ru(CO)2(C5H5))}

Guidance literature:

In toluene; solid carbonylmetal salt is added to a soln. of the Ti-complex in toluene at -70°C, the mixture is warmed to room temp. over 20 h; the solvent is removed in vac., the residue is extd., the extract is filtd., the solvebt is evapd., the residue is washed (cold pentane), elem. anal.;

Reference yield: 61.0%

potassium cyclopentadienyldicarbonyliron(0) + {HC{Si(CH3)2NC6H4CH3}3TiBr} (156053-53-1) → {HC{Si(CH3)2NC6H4CH3}3Ti(Fe(CO)2(C5H5))}

Guidance literature:

In toluene; solid carbonylmetal salt is added to a soln. of the Ti-complex in toluene at -70°C, the mixture is warmed to room temp. over 20 h; the solvent is removed in vac., the residue is extd., the extract is filtd., the solvebt is evapd., the residue is washed (cold pentane), elem. anal.;

upstream raw materials:

TiBr₄(THF)2

Downstream raw materials:

{HC{Si(CH₃)2NC₆H₄CH₃}3Ti(Co(CO)3(P(C₆H₅)3))}

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