Technology Process of C54H66O8S2
There total 6 articles about C54H66O8S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
5-dodecylthiophene-2-carboxylic acid; 1,3-phenylene bis(4-hydroxybenzoate);
With
dmap;
In
dichloromethane;
for 0.166667h;
With
N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate;
In
dichloromethane;
at 20 ℃;
for 24h;
DOI:10.1039/c0jm01919d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dmap; triethylamine / dichloromethane / 4 h / Inert atmosphere
2.1: palladium 10% on activated carbon; hydrogen / 1,4-dioxane / 40 °C / 2025.2 Torr
3.1: dmap / dichloromethane / 0.17 h
3.2: 24 h / 20 °C
With
dmap; palladium 10% on activated carbon; hydrogen; triethylamine;
In
1,4-dioxane; dichloromethane;
DOI:10.1039/c0jm01919d
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / diethyl ether; hexane / Inert atmosphere; Cooling with ice; Reflux
1.2: 20 °C / Inert atmosphere
2.1: dmap / dichloromethane / 0.17 h
2.2: 24 h / 20 °C
With
dmap; n-butyllithium;
In
diethyl ether; hexane; dichloromethane;
DOI:10.1039/c0jm01919d