Technology Process of C15H15NO8
There total 6 articles about C15H15NO8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: methanol; potassium carbonate
2: 1,2-dichloro-ethane
3: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Reflux
4: ozone / dichloromethane
5: sodium tetrahydroborate
6: 4-methyl-morpholine
With
4-methyl-morpholine; methanol; sodium tetrahydroborate; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; potassium carbonate; ozone;
In
dichloromethane; 1,2-dichloro-ethane; toluene;
DOI:10.1002/cmdc.201000318
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1,2-dichloro-ethane
2: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Reflux
3: ozone / dichloromethane
4: sodium tetrahydroborate
5: 4-methyl-morpholine
With
4-methyl-morpholine; sodium tetrahydroborate; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; ozone;
In
dichloromethane; 1,2-dichloro-ethane; toluene;
DOI:10.1002/cmdc.201000318
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Reflux
2: ozone / dichloromethane
3: sodium tetrahydroborate
4: 4-methyl-morpholine
With
4-methyl-morpholine; sodium tetrahydroborate; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; ozone;
In
dichloromethane; toluene;
DOI:10.1002/cmdc.201000318
