C₆H₅ONi(P(C₆H₁₁-cyclo)3)2H

Base Information

Chemical Name:C₆H₅ONi(P(C₆H₁₁-cyclo)3)2H
CAS No.:25703-58-6
Molecular Formula:C₄₂H₇₂NiOP₂
Molecular Weight:713.671
Hs Code.:

C<sub>6</sub>H<sub>5</sub>ONi(P(C<sub>6</sub>H<sub>11</sub>-cyclo)3)2H

Synonyms:

Suppliers and Price of C₆H₅ONi(P(C₆H₁₁-cyclo)3)2H

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆H₅ONi(P(C₆H₁₁-cyclo)3)2H

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆H₅ONi(P(C₆H₁₁-cyclo)3)2H

There total 3 articles about C₆H₅ONi(P(C₆H₁₁-cyclo)3)2H which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 22829-35-2,25703-57-5
trans-Ni(Cl)(H)(PCy₃)2

: 139-02-6
sodium phenoxide

: 25703-58-6,120294-42-0
C₆H₅ONi(P(C₆H₁₁-cyclo)3)2H

Guidance literature:: In tetrahydrofuran; benzene; (N2 atmosphere, Schlenk technique); to a soln. of Ni-compd. in THF and benzene at room temp. is added an excess of NaOPh, soln. is stirred for 1 h; solvent is removed under vac., residue is extd. with toluene, filtrate is concd., cooled to -20°C, crystn.; elem. anal.;

Reference yield: 55.0%

: [Ni(PCy₃)2]2(N₂)

: 25703-58-6,120294-42-0
C₆H₅ONi(P(C₆H₁₁-cyclo)3)2H

Guidance literature:: With C₆H₅OH; In diethyl ether; toluene; (Ar); to Ar-purged (1 h) concd. soln. of Ni complex was added phenol soln. in ether resulting pptn.; pptn. was filtered, washed with ether and dried in vac.; elem. anal.;

Reference yield:

: 2622-14-2
tricyclohexylphosphine

: 25703-58-6,120294-42-0
C₆H₅ONi(P(C₆H₁₁-cyclo)3)2H

Guidance literature:: Multi-step reaction with 2 steps

1: toluene

2: C₆H₅OH / diethyl ether; toluene

With C₆H₅OH; In diethyl ether; toluene;