{Os₃(CO)11(P(CH₃)2C₆H₅)}

Base Information

Chemical Name:{Os₃(CO)11(P(CH₃)2C₆H₅)}
CAS No.:98301-24-7
Molecular Formula:C₁₉H₁₁O₁₁Os₃P
Molecular Weight:1016.86
Hs Code.:

{Os<sub>3</sub>(CO)11(P(CH<sub>3</sub>)2C<sub>6</sub>H<sub>5</sub>)}

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {Os₃(CO)11(P(CH₃)2C₆H₅)}

Chemical Property:

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Technology Process of {Os₃(CO)11(P(CH₃)2C₆H₅)}

There total 4 articles about {Os₃(CO)11(P(CH₃)2C₆H₅)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 12775-47-2,90758-92-2,95404-11-8,95404-12-9,98302-16-0
Os₃(CO)10(P(CH₃)2(C₆H₅))2

: 12775-47-2,90758-92-2,95404-11-8,95404-12-9,98302-16-0
Os₃(CO)10(P(CH₃)2(C₆H₅))2

: 12775-47-2,90758-92-2,95404-11-8,95404-12-9,98302-16-0
Os₃(CO)10(P(CH₃)2(C₆H₅))2

: Os₃(CO)9(P(CH₃)2(C₆H₅))3

: {Os₃H(CO)9(Me₂PC₆H₄-o)(PMe₂Ph)}

: 98301-24-7
Os₃(CO)11(P(CH₃)2(C₆H₅))

Guidance literature:: In toluene; soln. of Os-complex in toluene was refluxed under Ar for 2 h; solvent removed under vac., sepd. by chromy. (t.l.c. (SiO2), eluant light petroleum-CH2Cl2); elem. anal.;

Reference yield: 5.1%

: 61817-93-4,146143-79-5,871132-66-0
bis(acetonitrile)decacarbonyltriosmium

: 672-66-2
Dimethyl(phenyl)phosphine

: 12775-47-2,90758-92-2,95404-11-8,95404-12-9,98302-16-0
Os₃(CO)10(P(CH₃)2(C₆H₅))2

: 98301-24-7
Os₃(CO)11(P(CH₃)2(C₆H₅))

Guidance literature:: In dichloromethane; soln. of 3 equiv of PMe2Ph and 1 equiv of Os-complex in CH2Cl2 stood at room temp. in the dark under N2 for 48 h; further products; solvent removed under vac., sepd. by chromy. (t.l.c. (SiO2), eluant light petroleum-CH2Cl2);

Reference yield:

: 89378-13-2
[Os₃(CO)10(P(CH₃)2C₆H₅)(CHO)]^(1-)

: 98301-24-7,36885-43-5
{Os₃(CO)11(P(CH₃)2C₆H₅)}

Guidance literature:: With phosphoric acid; In tetrahydrofuran; under N2, excess deoxygenated 20% H3PO4 added dropwise to THF soln. of educt; extd. with CH2Cl2, dried over anhyd. MgSO4, filtered, evapd.;
DOI:10.1021/ja00321a601